MSE672: Introduction to TEM


1.5. Course Organization#

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MSE672: Introduction to Transmission Electron Microscopy

Spring 2024

Gerd Duscher Khalid Hattar
Microscopy Facilities Tennessee Ion Beam Materials Laboratory
Materials Science & Engineering Nuclear Engineering
Institute of Advanced Materials & Manufacturing
The University of Tennessee, Knoxville

1.5.1. Books#

1.5.1.1. Williams and Carter#

Transmission Electron Microscopy

Plenum Press, 2009 (2nd Edition).

available online at the library

1.5.1.2. Reimer and Kohl#

Transmission Electron Microscopy

Springer, Berlin, 2007 (5th Edition).

available online at the library

1.5.1.3. Zuo and Spence#

Advanced Transmission Electron Microscopy: Imaging and Diffraction

Springer, NewYork, 2017

available online at the library

1.5.1.4. Kirkland#

Advanced Computing in Electron Microscopy

Springer, NewYork, 2010 (2nd Edition)

available online at the library

1.5.1.5. R.F. Egerton#

Electron Energy-Loss Spectroscopy in the Electron Microscope

Plenum Press, 2011 (3rd Edition)

available online at the library

1.5.2. Software#

1.5.2.1. Image Analysis software for SEM and TEM#

1.5.2.1.1. Digital Micrograph#

You can get a free offline license from Gatan

1.5.2.1.2. ImageJ#

a free imaging software with a lot of plugins: download from NIH

1.5.2.1.3. jupyter notebooks#

use provided notebooks

1.5.3. Syllabus#

Week

Lecture

Chp.

Lab

01/22 - 01/28

1,2:Introduction, Geometric Ray Optics

1

01/29 - 02/04

3,4: Kinematic Diffraction

2,11

Lab1: Basic Imaging

02/05 - 02/11

5,6:Kinematic Diffraction -parallel

12

Lab2: Basic Diffraction

02/12 - 02/18

7,8:Kinematic Diffraction -convergent

19,20

Lab3: SAED

02/19 - 02/25

9,10:Dynamic Diffraction

14,15

Lab4: CBED

02/26 - 03/03

11,12:Imaging Overview

22

Lab5: Two Beams

03/04 - 03/10

13,14:Imaging Conventional

24-27

Lab7: Phase Contrast

03/18 - 03/24

15,16:Imaging Phase Contrast

28,30

Lab6: Exam Preparation

03/25 - 03/31

17,18:Imaging and Lens Aberrations

31

Exam

04/01 - 04/07

19 :Imaging Z-contrast

-

Lab8: CTF

04/08 - 04/14

20,21:Spectroscopy EELS

36-40

Lab9: Z-contrast

04/15 - 04/21

22,23:Spectroscopy EDS

33-35

Lab10: EELS, ESI

04/22 - 04/28

24:Other Techniques

29

04/29 - 05/05

25,26: TEM parts and vacuum

5-9

05/06 -

28:Project discussion

1.5.4. Office Hours#

Office hours are Thursday from 2 – 4pm online with the class zoom link.

I will answer email questions in the same time slots.

1.5.5. Class and Lab#

  • Parallel to the class there is a Lab (MSE676) course.

  • We will analyze the data of the lab course, independent of whether you are participating or not,

  • For the analysis of the data we will need a labtop in class.

  • Everyone needs a laptop in class

  • I need real feedback on what you guys want to do and need to learn.

1.5.6. Homework and Quizzes#

  • Homeworks and Quizzes are the main way to determine your grade in this course.

  • Homeworks have to be submitted electronically through Canvas and generally are about analyzing on your own data which are similar to those in the practice sessions.

  • Think of these homeworks as small take-home exams.

  • Additionally, there will be reading assignments every week.

  • Each week before the lecture, there will be a short quiz about the content of the reading assignments.

  • Neither the TA nor the instructor will answer questions about your homework after the deadline.

  • If you are more than two homeworks behind, you failed the class.

1.5.7. Final#

The final is a report of how TEM will/can be used in your research. This should include a critical review of data from journal articles which did TEM similar to what you propose.

1.5.8. Grades#

The grade is a determined by 1/3 each: final, homework, and quizzes.